Table of Contents
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Index
Malfunctions. See Symptoms of malfunctions
Manual tune, 48
Mass assignments, incorrect, 76
Mass filter
219 width, 224
amu gain, 223
amu offset, 224
dc polarity, 225
dc voltage, 223
difficulty with the mass filter electronics, 84
heater, 230
heater and sensor, reinstalling, 168
heater and sensor, removing, 166
maintenance, 226
mass (axis) gain, 225
mass (axis) offset, 225
parameters, 223
radiator, 230
RF voltage, 223
Mass filter temperature
monitor, 38
setting, 40
viewing, 36
Mass gain, 225
Mass offset, 225
Mass spectra
high abundances at m/z 18, 28, 32, and 44 or at
m/z 14 and 16, 75
high background, 75
inconsistent peak widths, 76
incorrect mass assignments, 76
isotopes missing or ratios are incorrect, 75
precursors, 76
288
Mass-to-charge ratio, 223
Monitoring
foreline pressure, 36
turbo pump speed, 36
vacuum manifold pressure, 44
Monitors, 38
Moving the MSD, 62
MS error numbers, 84
MSD
dangerous voltages in, 97
dangerously hot parts in the, 98
does not turn on, 68
electronics, 233 – ??
hazards from chemical residue, 99
interfacing to external devices, 248
maintaining, 93 – ??
measuring column flow with the, 46
moving or storing, 62
operating, 31 – ??
troubleshooting, 65 – 92
MSD ChemStation. See ChemStation
N
Noise declaration, inside front cover
O
Oil trap, 194
replacing, 108
On/off switch. See Power switch
Opening the vacuum manifold, 54
Operating the MSD, 31 – ??
Ordering parts, 254
O-rings and O-ring assemblies, 192
part numbers, 260
Oxygen, effect of on column bleed, 18
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